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  1. Abstract

    In recent years Bi2Sr2CaCu2Ox(Bi-2212) received increasing attention due to its round wire multifilamentary architecture, a unique feature in high-Tcsuperconductor. In fact, round wires are preferable for magnet designs, including solenoids for nuclear magnetic resonance (NMR) or research purpose and accelerator magnets. However, due to the narrow over-pressure heat treatment conditions necessary to obtain highJcand to the peculiar microstructure of Bi-2212 wires, a full understanding of the correlations between the different properties has not yet been developed. In this paper we investigate the effect of a vital part of Bi-2212 optimization, the maximum heat-treatment temperatureTmaxin the range of 885 °C–896 °C, on the variations ofJc, effective filament diameterdeff, anisotropyγ, INTER- and intra-grain irreversibility fields and pinning energiesU0, all critical parameters in unravelling the complex mix of vortex pinning and connectivity that ultimately determines the critical current density. We found thatdeffof the higherJcwires heat-treated at lower temperature is much smaller than for the lowerJcwires. Moreover, a systematic increase of the irreversibility field and a decrease of the intrinsic Bi-2212 anisotropy underpins the higherJc. The analysis of the pinning energies reveals that there is little sample-to-sample variation in the INTER-grain pinning, whereas in all samples the intra-grain pinning has an enhancement below ∼40–45 K becoming more and more evident with increasingJc. These results suggest that the overallJcperformance are not only related to the wire microstructure and connectivity, which obviously affect the INTER-grain properties, but they are also intimately related to the intrinsic and intra-grain properties such asγandU0.

     
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  2. Abstract

    Although nanoscale deformation, such as nanostrain in iron-chalcogenide (FeSexTe1−x, FST) thin films, has attracted attention owing to its enhancement of general superconducting properties, including critical current density (Jc) and critical transition temperature, the development of this technique has proven to be an extremely challenging and complex process thus far. Herein, we successfully fabricated an epitaxial FST thin film with uniformly distributed nanostrain by injection of a trace amount of CeO2inside an FST matrix using sequential pulsed laser deposition. By means of transmission electron microscopy and geometric phase analysis, we verified that the injection of a trace amount of CeO2forms nanoscale defects, with a nanostrained region of tensile strain (εzz ≅ 0.02) along thec-axis of the FST matrix. This nanostrained FST thin film achieves a remarkableJcof 3.5 MA/cm2under a self-field at 6 K and a highly enhancedJcunder the entire magnetic field with respect to those of a pristine FST thin film.

     
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